REFMAC

TLS
RANGE  'A   3.' 'A  99.' ALL
ORIGIN    32.1706  30.6880  43.5682
T     1.5374   1.3722   1.2298   0.1027  -0.0274  -0.1283
L    17.4556  15.1358  27.5669   6.6344   9.4081  11.9175
S     0.2713   0.3072   0.4546  -1.2407  -0.4570  -0.9909   1.2373   0.3187
TLS
RANGE  'A 100.' 'A 284.' ALL
ORIGIN     8.4983  15.7677   3.0037
T     0.2874   0.2670   0.3604   0.0038   0.1006  -0.0024
L     3.0507   2.7362   1.9824  -1.1244   0.6576  -1.7643
S    -0.0432  -0.0691  -0.1745   0.1215  -0.0381   0.1558  -0.1412   0.0402