REFMAC TLS RANGE 'B 1.' 'B 8.' ALL ORIGIN 5.2300 14.1480 20.8078 T 0.1161 0.1006 0.1338 -0.0196 0.0145 0.0159 L 6.0151 4.1403 0.0446 -1.9239 0.4483 -0.3420 S 0.0197 -0.0902 -0.1787 0.0736 -0.1645 0.0996 -0.1413 0.0121 TLS RANGE 'B 9.' 'B 30.' ALL ORIGIN 16.8244 5.1431 18.6819 T 0.2008 0.1885 0.1558 0.0040 -0.0031 -0.0078 L 3.4412 1.6092 0.7863 0.4029 -0.0637 -0.0766 S 0.0112 -0.0475 0.1100 0.0949 -0.3936 -0.1401 -0.0781 0.3406 TLS RANGE 'B 31.' 'B 64.' ALL ORIGIN 19.8862 -7.5711 14.9495 T 0.2039 0.1837 0.1814 0.0010 0.0138 0.0139 L 2.9398 1.3807 1.7663 0.4640 1.0373 0.8429 S 0.0083 0.0581 0.0247 -0.0372 -0.2263 0.0559 0.0167 0.2164 TLS RANGE 'B 65.' 'B 99.' ALL ORIGIN 14.7054 2.1345 23.7078 T 0.1419 0.1285 0.1445 -0.0072 -0.0033 0.0091 L 0.9429 0.7258 1.2899 -0.4697 -0.6330 0.4829 S 0.0241 0.0092 -0.0241 0.1079 -0.0746 -0.0064 -0.1334 0.0829