REFMAC TLS RANGE 'B 1.' 'B 24.' ALL ORIGIN 14.1768 10.0935 18.9439 T 0.1964 0.1535 0.1672 -0.0191 -0.0004 0.0067 L 5.0974 1.7471 1.1513 -1.4855 0.2566 -0.0979 S -0.0462 0.0786 0.0832 0.1401 -0.2972 -0.0302 0.1053 0.2627 TLS RANGE 'B 25.' 'B 76.' ALL ORIGIN 18.9509 -4.8345 17.8567 T 0.1919 0.1744 0.1791 -0.0039 0.0049 0.0224 L 1.1697 0.9473 1.3863 -0.1090 0.1100 0.8124 S 0.0585 0.0572 0.0304 -0.0298 -0.2130 0.0008 0.0084 0.2277 TLS RANGE 'B 77.' 'B 99.' ALL ORIGIN 11.6074 1.8845 22.8478 T 0.1135 0.1033 0.1223 -0.0120 -0.0049 0.0060 L 1.5120 1.0532 0.7089 -0.7247 -0.7299 0.5651 S -0.0179 0.0302 0.0190 0.0411 0.0152 -0.0243 -0.1175 -0.0985