REFMAC

TLS
RANGE  'B   1.' 'B  24.' ALL
ORIGIN    14.1768  10.0935  18.9439
T     0.1964   0.1535   0.1672  -0.0191  -0.0004   0.0067
L     5.0974   1.7471   1.1513  -1.4855   0.2566  -0.0979
S    -0.0462   0.0786   0.0832   0.1401  -0.2972  -0.0302   0.1053   0.2627
TLS
RANGE  'B  25.' 'B  99.' ALL
ORIGIN    16.7284  -2.8010  19.3673
T     0.1612   0.1439   0.1570  -0.0063  -0.0008   0.0201
L     1.0073   0.9893   1.5075  -0.1795  -0.2064   0.6584
S     0.0450   0.0411   0.0306  -0.0079  -0.1715  -0.0247   0.0215   0.1928