REFMAC

TLS
RANGE  'A   1.' 'A   8.' ALL
ORIGIN     4.2703  -0.2221  31.6917
T     0.1923   0.1987   0.1959  -0.0174   0.0026   0.0218
L     3.9397   7.1960   5.6296  -4.2707  -2.8280   2.4058
S    -0.0348  -0.1513  -0.0362  -0.2690   0.1236   0.2882   0.4426  -0.0827
TLS
RANGE  'A   9.' 'A  99.' ALL
ORIGIN    -6.8956   2.1190  16.2094
T     0.1324   0.1241   0.1390   0.0010   0.0025   0.0120
L     1.1099   1.3880   1.5482  -0.0144  -0.0398   0.3880
S    -0.0157  -0.0175   0.0567  -0.0772   0.1533  -0.0524   0.0665  -0.1786