REFMAC

TLS
RANGE  'A   1.' 'A 115.' ALL
ORIGIN   -30.2619 -20.4658   5.9621
T     0.0720   0.0570   0.0581   0.0002   0.0029  -0.0096
L     1.1212   0.6681   0.6054   0.0844  -0.0793  -0.0748
S    -0.0162  -0.0181   0.0017  -0.0057  -0.0615   0.0011   0.0022   0.0532
TLS
RANGE  'A 116.' 'A 298.' ALL
ORIGIN   -35.8504 -17.2905  33.5279
T     0.0730   0.0697   0.1070   0.0052   0.0088  -0.0086
L     0.4701   0.4450   1.0419  -0.0074   0.0970  -0.1496
S    -0.0102   0.0004  -0.0691  -0.0017  -0.0042   0.0483   0.0012  -0.0098
TLS
RANGE  'A 299.' 'A 346.' ALL
ORIGIN   -35.5609  -9.4196  20.2982
T     0.0817   0.0861   0.0868   0.0041  -0.0104  -0.0107
L     0.4905   1.1117   1.1337   0.6871  -0.6037  -1.0871
S    -0.1245   0.1999  -0.0634   0.1070   0.0634   0.1101  -0.1770   0.0398