REFMAC

TLS
RANGE  'A   1.' 'A 299.' ALL
ORIGIN   -33.7007 -18.4685  22.9925
T     0.0722   0.0591   0.1020  -0.0011  -0.0005  -0.0005
L     0.3123   0.2294   0.8126  -0.0053  -0.0243   0.0218
S     0.0045  -0.0037  -0.0246   0.0067  -0.0013   0.0188  -0.0109   0.0089
TLS
RANGE  'A 300.' 'A 346.' ALL
ORIGIN   -35.7736  -9.4135  20.6922
T     0.0834   0.0876   0.0865   0.0028  -0.0097  -0.0111
L     0.4562   1.1434   1.1717   0.6888  -0.6357  -1.1317
S    -0.1277   0.2086  -0.0705   0.1124   0.0703   0.1134  -0.1783   0.0393