REFMAC

TLS
RANGE  'A   8.' 'A  37.' ALL
ORIGIN    90.7465  32.7581  65.9617
T     0.1582   0.2231   0.1626   0.0116   0.0045   0.0250
L     1.5169   8.0640   2.7609   1.1453   0.5707   3.2515
S     0.0889   0.0639  -0.0174   0.0112  -0.1921   0.0857   0.0070   0.0856
TLS
RANGE  'A  38.' 'A 116.' ALL
ORIGIN    94.1876  32.5982  55.6566
T     0.1984   0.2159   0.1757   0.0077   0.0142   0.0060
L     0.9726   1.5524   0.5542   0.6264   0.3312   0.4299
S     0.0069   0.0654  -0.0235  -0.0317  -0.2250   0.0927  -0.0259   0.1237
TLS
RANGE  'A 117.' 'A 135.' ALL
ORIGIN    90.4268  52.7652  61.0949
T     0.2138   0.2581   0.2055   0.0272  -0.0052   0.0150
L     4.4862   8.9505   2.1903   3.9027   0.1297   0.2138
S     0.0626  -0.0358  -0.1332   0.3727  -0.0548   0.0046  -0.3901   0.2372
TLS
RANGE  'A 136.' 'A 225.' ALL
ORIGIN    76.2020  36.8824  55.0620
T     0.1481   0.1678   0.1731   0.0020  -0.0006   0.0069
L     0.4275   0.7542   1.2110  -0.0750  -0.0020   0.4179
S    -0.0172  -0.0087  -0.0385   0.0484   0.0784   0.0478  -0.0523  -0.0739
TLS
RANGE  'A 226.' 'A 267.' ALL
ORIGIN    84.4566  26.3147  43.4223
T     0.1168   0.1742   0.1465   0.0381  -0.0065  -0.0061
L     1.6016   2.3038   1.7040   0.8056  -0.3636  -0.7321
S     0.0173   0.0238   0.0196   0.0384  -0.0080  -0.0068  -0.0438   0.0368
TLS
RANGE  'A 268.' 'A 289.' ALL
ORIGIN    89.7599  28.0615  38.9968
T     0.1458   0.1542   0.1660   0.0149   0.0357   0.0055
L     2.6410   1.5725   4.2431   0.9499   2.5845   1.1071
S    -0.0376   0.0569  -0.0101  -0.0433  -0.0041   0.0199   0.0799   0.0089
TLS
RANGE  'A 290.' 'A 309.' ALL
ORIGIN    68.8211  27.0043  41.2507
T     0.1502   0.1776   0.1863  -0.0068  -0.0107   0.0284
L     2.5828   2.9553   3.6046   0.8801   0.8340  -0.0853
S    -0.0914   0.0107   0.0178   0.0877   0.0830  -0.0777  -0.1976  -0.1241