REFMAC

TLS
RANGE  'B   1.' 'B  15.' ALL
ORIGIN    13.9483  17.3135  20.1837
T     0.2003   0.1514   0.2198  -0.0260   0.0119   0.0016
L     6.1878   2.1500   1.7161  -2.1510   0.2383   0.0011
S     0.0604  -0.0144  -0.0303  -0.3956   0.3139   0.1278   0.1111  -0.1384
TLS
RANGE  'B  16.' 'B  99.' ALL
ORIGIN     8.6157  30.4415  18.8765
T     0.1816   0.1714   0.1760   0.0153   0.0078   0.0076
L     1.5392   1.3275   0.9736  -0.2787  -0.2959  -0.3256
S     0.1516   0.0205  -0.0211  -0.0495   0.2345   0.0502   0.0253  -0.1545