REFMAC TLS RANGE 'A 1.' 'A 99.' ALL ORIGIN 30.8557 27.2638 17.7819 T 0.1649 0.1538 0.1779 0.0065 -0.0170 0.0051 L 1.4441 1.2697 1.3695 -0.0293 0.0160 -0.2161 S -0.0113 -0.0974 -0.0488 0.0230 -0.1963 0.0802 -0.0748 0.1732