REFMAC

TLS
RANGE  'A   2.' 'A  73.' ALL
ORIGIN    -5.8173   0.0407  18.1022
T     0.1046   0.0316   0.1006  -0.0089  -0.0162  -0.0202
L     1.3873   1.3724   2.0080   0.0790  -0.1793  -0.4423
S     0.1181  -0.1012  -0.0100   0.0441  -0.0964  -0.0805  -0.0257   0.0271
TLS
RANGE  'A  74.' 'A  80.' ALL
ORIGIN   -21.2403  12.3175  15.7446
T     0.1592   0.2085   0.3035   0.0137  -0.0984   0.0113
L     1.1207  34.5925  12.2308   3.0573  -3.4906 -15.4948
S     0.6539   0.3112   0.1340   0.7075   0.8942  -1.1067  -0.1308  -0.7966
TLS
RANGE  'A  81.' 'A 260.' ALL
ORIGIN   -10.5383  -2.9409  15.2640
T     0.0782   0.0702   0.0766  -0.0101  -0.0059   0.0147
L     1.0794   1.3822   1.3027  -0.1452   0.0363   0.1887
S     0.0262   0.0232   0.0203  -0.0394   0.0361  -0.1192  -0.0016  -0.0299