REFMAC

TLS
RANGE  'A   2.' 'A  80.' ALL
ORIGIN    -7.2023   1.1431  17.8905
T     0.1138   0.0276   0.1021  -0.0147  -0.0228  -0.0164
L     1.4967   1.3930   2.0886   0.1483  -0.1799  -0.3451
S     0.1543  -0.1238   0.0040   0.0984  -0.0512  -0.0939  -0.0844  -0.0212
TLS
RANGE  'A  81.' 'A 260.' ALL
ORIGIN   -10.5383  -2.9409  15.2640
T     0.0782   0.0702   0.0766  -0.0101  -0.0059   0.0147
L     1.0794   1.3822   1.3027  -0.1452   0.0363   0.1887
S     0.0262   0.0232   0.0203  -0.0394   0.0361  -0.1192  -0.0016  -0.0299