REFMAC

TLS
RANGE  'A   2.' 'A 260.' ALL
ORIGIN    -9.5045  -1.6752  16.0779
T     0.0844   0.0680   0.0843  -0.0040  -0.0088   0.0139
L     1.1086   1.4201   1.3993  -0.0030   0.0241   0.1022
S     0.0544  -0.0152   0.0154   0.0092   0.0121  -0.1109  -0.0433  -0.0342