REFMAC TLS RANGE 'B 1.' 'B 52.' ALL ORIGIN 23.9309 28.9294 132.0157 T 0.4903 0.5097 0.5349 -0.0066 0.0183 -0.0030 L 0.4954 1.3482 2.8184 0.1551 0.2009 0.0173 S -0.0365 -0.0009 -0.1554 -0.0987 -0.2234 0.2162 0.1215 0.2414 TLS RANGE 'B 53.' 'B 101.' ALL ORIGIN 36.6586 43.2470 120.5309 T 0.5070 0.4933 0.5030 -0.0066 -0.0131 0.0232 L 1.1610 1.6740 1.4336 -0.3919 -0.0577 0.8542 S 0.0550 -0.0187 0.0579 -0.0780 -0.1037 -0.0777 0.0643 0.1218