REFMAC

TLS
RANGE  'M   2.' 'M 138.' ALL
ORIGIN    99.6637  37.3888  44.6270
T     0.5241   0.5225   0.4827  -0.0024  -0.0138   0.0034
L     1.2077   0.8988   0.7524  -0.4265  -0.1583   0.0009
S    -0.0395   0.0177  -0.1675   0.0257  -0.0082   0.1422  -0.0450   0.0541
TLS
RANGE  'M 139.' 'M 395.' ALL
ORIGIN    99.9465  45.2557  78.7159
T     1.5583   1.5650   1.5482  -0.0062   0.0165  -0.0216
L     0.4483   0.8252   0.7499  -0.6019   0.3706  -0.5846
S     0.0471   0.0450  -0.3667  -0.3520  -0.0260   0.2828   0.2632   0.0088
TLS
RANGE  'M 396.' 'M 526.' ALL
ORIGIN   101.4612  50.5690  42.8679
T     0.5476   0.5759   0.5524  -0.0288  -0.0005   0.0031
L     1.0495   1.6108   0.7588  -0.7052   0.0905   0.1466
S     0.0002   0.0150  -0.1300   0.1667   0.0540   0.1258  -0.1213  -0.0600