REFMAC

TLS
RANGE  'J   2.' 'J  78.' ALL
ORIGIN    88.8673 -32.7190  44.9722
T     0.5538   0.5204   0.5163  -0.0119   0.0056   0.0060
L     2.9995   0.5807   0.3184  -1.0790   0.0041  -0.2490
S     0.0305  -0.0484  -0.1611   0.0654   0.0022   0.1200  -0.0876   0.0179
TLS
RANGE  'J  79.' 'J 156.' ALL
ORIGIN    87.0188 -53.2615  47.3350
T     0.6213   0.6088   0.5896  -0.0113   0.0511  -0.0274
L     1.4741   1.7108   1.5381  -0.3443   0.5059  -0.4799
S     0.0022   0.0391  -0.2530  -0.1836  -0.2010   0.2426   0.1745   0.1592
TLS
RANGE  'J 157.' 'J 395.' ALL
ORIGIN    89.1087 -46.5229  79.6869
T     1.4544   1.4473   1.4344  -0.0099  -0.0231   0.0092
L     1.2177   0.4373   0.9496  -0.6739  -0.4779   0.3668
S    -0.0271   0.0703  -0.1785   0.2139   0.1921   0.1879  -0.1551  -0.1973
TLS
RANGE  'J 396.' 'J 526.' ALL
ORIGIN    89.8890 -53.0351  42.6414
T     0.5713   0.5450   0.5479  -0.0281   0.0031  -0.0025
L     1.6970   0.9982   0.8408  -0.5868   0.0353  -0.1945
S     0.0150   0.0025  -0.0948  -0.0826  -0.1559   0.1182   0.0714   0.1006