REFMAC

TLS
RANGE  'J   2.' 'J 138.' ALL
ORIGIN    85.8188 -40.3978  44.4658
T     0.5458   0.5401   0.5067  -0.0004   0.0082   0.0006
L     1.2010   0.5625   0.5633  -0.1468   0.0318  -0.0026
S    -0.0244   0.0123  -0.1466  -0.0049  -0.0291   0.1502   0.0221   0.0016
TLS
RANGE  'J 139.' 'J 395.' ALL
ORIGIN    90.1372 -47.4696  78.3693
T     1.4219   1.4230   1.4157  -0.0088  -0.0281   0.0161
L     0.9278   0.4959   1.0120  -0.6668  -0.6297   0.5513
S    -0.0232   0.0645  -0.2336   0.2314   0.2116   0.2257  -0.1760  -0.1945
TLS
RANGE  'J 396.' 'J 526.' ALL
ORIGIN    89.8890 -53.0351  42.6414
T     0.5713   0.5450   0.5479  -0.0281   0.0031  -0.0025
L     1.6970   0.9982   0.8408  -0.5868   0.0353  -0.1945
S     0.0150   0.0025  -0.0948  -0.0826  -0.1559   0.1182   0.0714   0.1006