REFMAC

TLS
RANGE  'I   2.' 'I 137.' ALL
ORIGIN    53.7275 -26.5288  45.0642
T     0.5122   0.5155   0.4764  -0.0027   0.0061  -0.0064
L     0.5761   1.2090   0.5748  -0.2722   0.0007  -0.0638
S    -0.0186   0.0092  -0.1666  -0.0126  -0.0303   0.1454   0.0221  -0.0066
TLS
RANGE  'I 138.' 'I 526.' ALL
ORIGIN    49.8724 -35.3933  67.2196
T     1.0186   1.0739   1.1005  -0.0036   0.0077  -0.0070
L     0.0142   0.2372   1.0332  -0.0577   0.0653  -0.2279
S     0.0052   0.0255  -0.4630   0.1704  -0.1547   0.5070  -0.0703   0.1222