REFMAC

TLS
RANGE  'H   2.' 'H 140.' ALL
ORIGIN    44.0535   7.0226  46.1546
T     0.4752   0.4759   0.4354   0.0005  -0.0065  -0.0109
L     0.8476   1.1458   0.6446   0.2164  -0.0333  -0.0437
S     0.0175  -0.0150  -0.1314  -0.0210  -0.0538   0.1218  -0.0004   0.0441
TLS
RANGE  'H 141.' 'H 526.' ALL
ORIGIN    36.2618   4.6655  68.1511
T     0.8913   0.8831   0.9425   0.0394   0.0036  -0.0126
L     0.2274   0.2453   0.9683   0.2312  -0.0763  -0.1757
S    -0.0607   0.0595  -0.4209   0.0061  -0.2581   0.4299  -0.0154   0.1535