REFMAC

TLS
RANGE  'F   2.' 'F 526.' ALL
ORIGIN    46.3420  30.5803  -7.4164
T     0.9384   0.9704   0.9983  -0.0114   0.0103  -0.0115
L     0.3119   0.5022   0.6383  -0.0610   0.2467  -0.3527
S    -0.0210   0.0135   0.6688  -0.0687  -0.0262  -0.6661   0.0684   0.0277