REFMAC

TLS
RANGE  'E   2.' 'E 139.' ALL
ORIGIN    44.0065  -9.9176   8.6779
T     0.4427   0.4433   0.4053  -0.0031   0.0021  -0.0065
L     0.8198   0.8747   0.4664  -0.3303   0.0419   0.0343
S     0.0240  -0.0187   0.1129   0.0229  -0.0914  -0.1043  -0.0065   0.0660
TLS
RANGE  'E 140.' 'E 526.' ALL
ORIGIN    34.2185  -8.3587 -13.0719
T     0.9835   0.9665   1.0275  -0.0449  -0.0020  -0.0099
L     0.3391   0.2866   0.8329  -0.3117   0.1045  -0.1068
S    -0.0731   0.0600   0.5879  -0.0068  -0.2736  -0.5878   0.0139   0.1520