REFMAC

TLS
RANGE  'D   2.' 'D 111.' ALL
ORIGIN    66.9000 -31.8638   7.9235
T     0.4721   0.4479   0.4409  -0.0031   0.0027  -0.0027
L     1.5863   0.4732   0.3524   0.1057  -0.1846   0.2488
S    -0.0042  -0.0316   0.1376   0.1105  -0.0573  -0.0807  -0.0996   0.0590
TLS
RANGE  'D 112.' 'D 285.' ALL
ORIGIN    61.0272 -38.8672 -18.2319
T     0.8515   0.8214   0.8628   0.0112   0.0083  -0.0247
L     0.0414   0.1682   0.9000  -0.0799   0.1543  -0.3652
S    -0.0374   0.0116   0.2854   0.3789  -0.1073  -0.1674  -0.3419   0.1803
TLS
RANGE  'D 286.' 'D 398.' ALL
ORIGIN    60.3353 -43.6039 -29.2716
T     0.7770   0.7865   0.7813  -0.0352  -0.0320   0.0030
L     1.3048   1.8176   1.4669  -0.6099   0.0034   0.1879
S    -0.1481   0.1367   0.1713   0.2781  -0.1473  -0.2204  -0.2858   0.0916
TLS
RANGE  'D 399.' 'D 526.' ALL
ORIGIN    58.7775 -47.0821   9.8371
T     0.4509   0.3984   0.4211   0.0117   0.0044  -0.0009
L     1.7085   0.4884   0.8584   0.1711   0.1735   0.0751
S    -0.0131   0.0365  -0.0576  -0.0118   0.0429   0.0099  -0.0068  -0.0046