REFMAC

TLS
RANGE  'D   2.' 'D 111.' ALL
ORIGIN    66.9000 -31.8638   7.9235
T     0.4721   0.4479   0.4409  -0.0031   0.0027  -0.0027
L     1.5863   0.4732   0.3524   0.1057  -0.1846   0.2488
S    -0.0042  -0.0316   0.1376   0.1105  -0.0573  -0.0807  -0.0996   0.0590
TLS
RANGE  'D 112.' 'D 526.' ALL
ORIGIN    60.1566 -42.6596 -12.8293
T     0.6996   0.6756   0.7409   0.0093   0.0039  -0.0001
L     0.2829   0.1364   0.9437  -0.0166   0.1726   0.1513
S    -0.0137   0.0317   0.2797   0.2598  -0.0720  -0.2332  -0.2537   0.0683