REFMAC

TLS
RANGE  'A   1.' 'A  95.' ALL
ORIGIN    15.6821 -10.8536  21.7202
T     0.2536   0.2423   0.2518  -0.0015  -0.0036   0.0104
L     0.9034   1.0353   1.3032   0.1119  -0.2019   0.3160
S     0.0125  -0.0151  -0.0824  -0.0691  -0.0010   0.0816   0.0685   0.0083
TLS
RANGE  'A  96.' 'A 166.' ALL
ORIGIN    18.7310   2.4295  23.6677
T     0.2658   0.2569   0.2808   0.0040  -0.0041  -0.0041
L     0.3548   0.1941   1.5772   0.1031  -0.4512  -0.3564
S    -0.0498   0.0241  -0.1028   0.0100  -0.0312   0.1025  -0.0600   0.1161
TLS
RANGE  'A 167.' 'A 351.' ALL
ORIGIN     3.4967   4.1142   0.9279
T     0.2233   0.2188   0.2184  -0.0119   0.0025   0.0037
L     0.6189   0.6459   0.4534  -0.2570   0.0862   0.0169
S    -0.0029  -0.0107  -0.0007  -0.0129   0.0221   0.0079   0.0199  -0.0087