REFMAC TLS RANGE 'A 3.' 'A 275.' ALL ORIGIN -30.8125 -14.4162 12.5135 T 0.1317 0.1240 0.1186 -0.0015 -0.0041 0.0018 L 0.4734 0.4862 0.4185 0.0422 -0.1949 0.0864 S -0.0003 -0.0007 -0.0001 0.0404 0.0711 -0.0111 -0.0416 -0.0622 TLS RANGE 'A 276.' 'A 356.' ALL ORIGIN -39.8171 -10.3361 11.4811 T 0.1532 0.1572 0.1192 -0.0093 0.0033 0.0015 L 0.7321 0.4556 0.3275 -0.0799 0.0723 -0.0552 S 0.0234 -0.0166 -0.0370 0.1120 0.0769 0.0277 -0.0893 -0.0756 TLS RANGE 'A 357.' 'A 376.' ALL ORIGIN -27.3789 -38.8905 -24.2279 T 0.1494 0.1258 0.1893 0.0246 -0.0202 0.0062 L 2.0107 0.9629 2.8938 0.2784 -1.2761 0.6619 S 0.0623 0.0023 0.1918 0.0307 -0.0203 -0.0449 0.0659 -0.1573