REFMAC

TLS
RANGE  'A   3.' 'A 356.' ALL
ORIGIN   -32.9203 -13.4611  12.2718
T     0.1400   0.1321   0.1201  -0.0044  -0.0036   0.0005
L     0.5238   0.4170   0.3513   0.0086  -0.1482   0.0657
S    -0.0046   0.0024   0.0042   0.0499   0.0730  -0.0095  -0.0539  -0.0699
TLS
RANGE  'A 357.' 'A 376.' ALL
ORIGIN   -27.3789 -38.8905 -24.2279
T     0.1494   0.1258   0.1893   0.0246  -0.0202   0.0062
L     2.0107   0.9629   2.8938   0.2784  -1.2761   0.6619
S     0.0623   0.0023   0.1918   0.0307  -0.0203  -0.0449   0.0659  -0.1573