REFMAC

TLS
RANGE  'A   3.' 'A 376.' ALL
ORIGIN   -32.6113 -14.8791  10.2366
T     0.1394   0.1351   0.1384  -0.0032  -0.0054   0.0085
L     0.2953   0.2809   0.3611  -0.0061  -0.1396   0.1252
S    -0.0279   0.0103  -0.0052   0.0378   0.0708  -0.0053  -0.0493  -0.0696