REFMAC

TLS
RANGE  'A   4.' 'A 104.' ALL
ORIGIN    12.8240  18.7061  11.9951
T     0.4307   0.3886   0.4152   0.0008   0.0601   0.0011
L     4.6176   1.4648   4.6815  -0.3559   3.2004  -0.0873
S    -0.0852   0.1471   0.0877  -0.3260   0.2760  -0.1939   0.2940  -0.2783
TLS
RANGE  'A 105.' 'A 182.' ALL
ORIGIN    35.4921  29.1594  44.9180
T     0.2753   0.2524   0.3010   0.0055   0.0366   0.0160
L     3.4341   2.1258   3.6683   0.5828   1.8972   0.9705
S     0.0118  -0.0336  -0.0576   0.0807  -0.0300   0.0558  -0.0923   0.0073