REFMAC

TLS
RANGE  'D   9.' 'D  85.' ALL
ORIGIN    57.6381  76.1182  14.0771
T     0.2172   0.2382   0.2199  -0.0074  -0.0069  -0.0078
L     0.6611   1.3927   0.7388  -0.3645   0.0212  -0.1875
S     0.0145  -0.0238  -0.1356  -0.1177  -0.0478   0.1652   0.0994   0.0589
TLS
RANGE  'D  86.' 'D 201.' ALL
ORIGIN    61.8692  79.7763  -1.9536
T     0.2016   0.2155   0.2122   0.0015   0.0066   0.0042
L     0.4375   0.7885   0.7139   0.0037   0.1396   0.1083
S     0.0235   0.0115   0.0957  -0.0398  -0.0643  -0.1081   0.0190   0.0696
TLS
RANGE  'D 202.' 'D 222.' ALL
ORIGIN    54.6941  60.2725   8.5400
T     0.2965   0.2860   0.2794  -0.0143  -0.0127  -0.0090
L     2.6657   3.3515   1.5885  -0.7625   0.8360  -0.8873
S     0.0307  -0.0421   0.0876  -0.2902  -0.2645  -0.1725   0.3125   0.2875