REFMAC

TLS
RANGE  'C   9.' 'C 244.' ALL
ORIGIN    13.3133  48.8635  66.2625
T     0.2106   0.2271   0.2291   0.0069   0.0037  -0.0017
L     0.6202   0.7115   0.7430   0.1517   0.0197  -0.0126
S     0.0021  -0.0051   0.0317   0.0814  -0.0356  -0.0262  -0.0924   0.0465