REFMAC

TLS
RANGE  'A   2.' 'A 100.' ALL
ORIGIN   -16.1352  24.3502   5.0050
T     0.1739   0.1890   0.1667  -0.0075   0.0107   0.0073
L     0.8097   1.3901   0.7978  -0.1422   0.0661   0.0847
S    -0.0071   0.0010   0.0106  -0.0919  -0.0026   0.0174   0.0875   0.0345
TLS
RANGE  'A 101.' 'A 135.' ALL
ORIGIN   -11.9455  38.5494   7.6179
T     0.1467   0.1585   0.1711   0.0021  -0.0187  -0.0069
L     0.6666   1.1339   1.3886   0.0521  -0.1122  -0.2386
S    -0.0067  -0.0344  -0.0355  -0.0174  -0.0499  -0.0061   0.0194   0.0984
TLS
RANGE  'A 136.' 'A 158.' ALL
ORIGIN    -4.0928  40.1853   9.4885
T     0.1364   0.1809   0.1906   0.0134  -0.0197   0.0010
L     3.2779   4.3872   3.8984   1.1245  -0.7793  -1.6707
S    -0.0507   0.0747   0.0602   0.0035  -0.2006  -0.0292  -0.0943   0.2247
TLS
RANGE  'A 159.' 'A 222.' ALL
ORIGIN     0.2462  25.6800   2.4136
T     0.3053   0.3166   0.3106   0.0062   0.0076   0.0153
L     0.8090   1.8622   1.6085   0.8033   0.7397   1.7307
S     0.1889   0.0393   0.2308  -0.1350  -0.1972  -0.1647   0.0702   0.1934