REFMAC TLS RANGE 'A 2.' 'A 118.' ALL ORIGIN -16.3288 26.2976 6.4721 T 0.1655 0.1855 0.1658 -0.0059 0.0073 0.0105 L 0.6363 1.3358 0.7834 -0.0461 0.0144 0.2451 S -0.0050 -0.0111 0.0084 -0.0731 0.0027 0.0219 0.0836 0.0267 TLS RANGE 'A 119.' 'A 158.' ALL ORIGIN -5.2600 39.6031 5.2883 T 0.1655 0.1855 0.2087 0.0124 0.0010 -0.0064 L 0.8732 1.2155 3.8737 0.3424 0.0668 -1.2562 S 0.0068 -0.0596 0.0348 -0.0223 -0.1559 -0.0675 0.0355 0.2551 TLS RANGE 'A 159.' 'A 222.' ALL ORIGIN 0.2462 25.6800 2.4136 T 0.3053 0.3166 0.3106 0.0062 0.0076 0.0153 L 0.8090 1.8622 1.6085 0.8033 0.7397 1.7307 S 0.1889 0.0393 0.2308 -0.1350 -0.1972 -0.1647 0.0702 0.1934