REFMAC

TLS
RANGE  'A   4.' 'A 280.' ALL
ORIGIN    70.2657  27.8043  44.6099
T     0.2780   0.2760   0.2700  -0.0014  -0.0021   0.0008
L     0.3740   0.3146   0.2800   0.0592   0.0196  -0.0460
S    -0.0046   0.0090  -0.0054   0.0838  -0.0318  -0.0046  -0.0760   0.0123
TLS
RANGE  'A 281.' 'A 434.' ALL
ORIGIN    60.5073  26.7453  26.2196
T     0.3069   0.3021   0.3123   0.0009  -0.0020   0.0005
L     0.0997   0.0915   0.2380   0.0116  -0.0590  -0.0010
S     0.0001  -0.0013   0.0591   0.0047   0.0478  -0.0449  -0.0157  -0.0718