REFMAC

TLS
RANGE  'A   4.' 'A 434.' ALL
ORIGIN    66.7183  27.4193  37.9246
T     0.2819   0.2763   0.2896  -0.0011  -0.0005  -0.0010
L     0.2239   0.2046   0.2920   0.0042  -0.0312  -0.0486
S    -0.0040  -0.0032   0.0141   0.0516   0.0089  -0.0193  -0.0585  -0.0058