REFMAC TLS RANGE 'B 1.' 'B 116.' ALL ORIGIN 40.4590 119.8480 80.1566 T 0.4236 0.4468 0.4375 -0.0143 0.0074 -0.0152 L 2.4938 2.8657 2.6411 -0.1451 0.2522 -0.0177 S 0.0161 -0.0279 -0.0404 0.2591 -0.0740 0.1225 -0.2734 0.0374 TLS RANGE 'B 117.' 'B 330.' ALL ORIGIN 22.7367 118.5634 58.8837 T 0.5459 0.4837 0.4657 -0.0349 0.0224 -0.0204 L 1.9718 1.7582 1.6385 -0.5467 0.8295 -0.4460 S 0.0080 -0.0044 0.1522 0.2386 0.1713 -0.0948 -0.2560 -0.2040 TLS RANGE 'B 331.' 'B 448.' ALL ORIGIN 21.9804 100.7706 76.6314 T 0.4100 0.3805 0.4385 -0.0299 0.0224 0.0289 L 1.9524 1.7993 2.9338 -0.2026 0.5701 0.4871 S 0.0002 -0.0125 -0.1245 0.0661 0.3170 0.0152 -0.1379 -0.4038