REFMAC

TLS
RANGE  'B   1.' 'B 448.' ALL
ORIGIN    27.2577 113.7780  69.6880
T     0.4547   0.4505   0.4614   0.0006   0.0341  -0.0181
L     0.8718   1.0476   1.3333  -0.0626   0.3392  -0.1607
S     0.0627  -0.0359   0.0244   0.1555   0.1235  -0.0431  -0.1722  -0.1360