REFMAC

TLS
RANGE  'A   2.' 'A 108.' ALL
ORIGIN    17.8430  45.0866  59.4448
T     0.1624   0.1758   0.1799  -0.0041   0.0071   0.0039
L     1.4484   1.3771   1.7763  -0.3763  -0.0362  -0.2770
S     0.0081   0.0257  -0.0843  -0.0910  -0.0933   0.1172   0.0892   0.0994
TLS
RANGE  'A 109.' 'A 294.' ALL
ORIGIN    10.8043  65.9963  49.1014
T     0.1628   0.1805   0.1533  -0.0207   0.0042   0.0034
L     0.7792   1.2282   0.6143  -0.3838  -0.0319   0.1205
S     0.0249  -0.0301  -0.0226   0.0857  -0.0884   0.0286  -0.0448   0.0438
TLS
RANGE  'A 295.' 'A 306.' ALL
ORIGIN     9.3665  52.0403  34.9912
T     0.4960   0.4662   0.4440  -0.0024   0.0194  -0.0272
L    17.7518  11.8220   9.9450  -7.2967   9.5110   0.1284
S    -0.0201   0.1106  -0.2677  -0.9485   0.4609  -0.1712   0.8468  -0.4725