REFMAC

TLS
RANGE  'A   2.' 'A 294.' ALL
ORIGIN    13.3578  58.4107  52.8538
T     0.1517   0.1846   0.1550  -0.0208   0.0076  -0.0109
L     0.6903   1.1409   0.6516  -0.3445   0.1274  -0.2418
S    -0.0005  -0.0207  -0.0214   0.0136  -0.0967   0.0436   0.0009   0.0621
TLS
RANGE  'A 295.' 'A 306.' ALL
ORIGIN     9.3665  52.0403  34.9912
T     0.4960   0.4662   0.4440  -0.0024   0.0194  -0.0272
L    17.7518  11.8220   9.9450  -7.2967   9.5110   0.1284
S    -0.0201   0.1106  -0.2677  -0.9485   0.4609  -0.1712   0.8468  -0.4725